{"id":1000,"date":"2021-11-22T12:12:07","date_gmt":"2021-11-22T12:12:07","guid":{"rendered":"http:\/\/www.calm-ebsd.com\/?page_id=1000"},"modified":"2021-12-10T21:03:03","modified_gmt":"2021-12-10T21:03:03","slug":"false-bands","status":"publish","type":"page","link":"https:\/\/www.calm-ebsd.com\/index.php\/how-to-start\/false-bands\/","title":{"rendered":"False bands"},"content":{"rendered":"\n<p>It can happen that, <strong>by chance<\/strong>, exactly where a band could be, an <strong>intensity accumulation <\/strong>occurs that actually <strong>looks<\/strong> <strong>like<\/strong> <strong>a band profile<\/strong>. <br><em>To make matters worse, <strong>most band profiles<\/strong> do not look as ideal as is commonly thought, but <strong>have a rather atypical<\/strong> <strong>shape<\/strong>. With CALM, you can inspect any profile after defining the band positions. <\/em><\/p>\n\n\n\n<p>Of course, it can also happen that <strong>single strong bands<\/strong> <strong>of another pattern<\/strong> become visible in one pattern because both <strong><a href=\"http:\/\/www.calm-ebsd.com\/index.php\/news\/possible-applications\/\" data-type=\"URL\" data-id=\"http:\/\/www.calm-ebsd.com\/index.php\/news\/possible-applications\/\"><span style=\"text-decoration: underline;\">superimpose<\/span><\/a><\/strong> in the image. These bands are <strong>usually easy to identify<\/strong> and are automatically ignored because they do not match the other bands, neither in direction nor in width.<br><em>The situation becomes <strong>more difficult when <a href=\"http:\/\/www.calm-ebsd.com\/index.php\/news\/possible-applications\/\" data-type=\"URL\" data-id=\"http:\/\/www.calm-ebsd.com\/index.php\/news\/possible-applications\/\"><span style=\"text-decoration: underline;\">crystallographic intergrowths<\/span><\/a> occur<\/strong> (e.g. single or multiple twinning) and such patterns overlap. There a separation can become difficult, especially if by chance both lattices generate a superlattice.<\/em><\/p>\n\n\n\n<p style=\"font-size:22px\">Wrong [hkl]* selected in a pattern from anatase (TiO<sub>2<\/sub>)<\/p>\n\n\n\n<p>It is not very difficult to describe a band position [hkl]*<sub>j<\/sub> by another very close [hkl]*<sub>i<\/sub>, e.g. by [3h<sub>i<\/sub> 3k<sub>i<\/sub> (3l<sub>i<\/sub>+1)]*. Depending on the (unknown) lattice parameters, the <strong>angular distance<\/strong> of [hkl]*<sub>i<\/sub> and [hkl]*<sub>j<\/sub><strong> can be<\/strong> as small as <strong>a few tenths of a degree<\/strong> only.<br><em><span style=\"text-decoration: underline;\">Please consider:<\/span><strong> During definition<\/strong> of the trace positions the <strong>indexing<\/strong> is totally <strong>unknown<\/strong>. High and low indexing of [hkl]* is later decided by their bandwidth. However, by visual inspection of the circles around [hkl]* you can predict how likely the defined pole might be, or whether there is another connection of two narrow bands (small circles) which might match better.<\/em><\/p>\n\n\n\n<p>Such an example is described in the following. In the left image below the uper right quarter of the Funk transformation of a Kukichi pattern from anatase is shown. Beside several ten poles <strong>one pole<\/strong> is <strong>displayed as red dot<\/strong>. It is defined by the intersection of two great circle. The one containing many [hkl]* is certainly reasonable. The other one, connecting one pole without and one with an intermediate band width (circle diameter) is only possibly reasonable       <\/p>\n\n\n\n<figure class=\"wp-block-gallery columns-3\"><ul class=\"blocks-gallery-grid\"><li class=\"blocks-gallery-item\"><figure><img loading=\"lazy\" width=\"388\" height=\"390\" src=\"http:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/wrongPole.png\" alt=\"\" data-id=\"967\" data-full-url=\"http:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/wrongPole.png\" data-link=\"http:\/\/www.calm-ebsd.com\/index.php\/news\/how-to-start\/manual-definition-of-bandwidths\/wrongpole\/\" class=\"wp-image-967\" srcset=\"https:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/wrongPole.png 388w, https:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/wrongPole-298x300.png 298w, https:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/wrongPole-150x150.png 150w, https:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/wrongPole-269x270.png 269w\" sizes=\"(max-width: 388px) 100vw, 388px\" \/><\/figure><\/li><li class=\"blocks-gallery-item\"><figure><img loading=\"lazy\" width=\"505\" height=\"188\" src=\"http:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/wrongBand.png\" alt=\"\" data-id=\"966\" data-full-url=\"http:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/wrongBand.png\" data-link=\"http:\/\/www.calm-ebsd.com\/index.php\/news\/how-to-start\/manual-definition-of-bandwidths\/wrongband\/\" class=\"wp-image-966\" srcset=\"https:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/wrongBand.png 505w, https:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/wrongBand-300x112.png 300w, https:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/wrongBand-360x134.png 360w\" sizes=\"(max-width: 505px) 100vw, 505px\" \/><\/figure><\/li><li class=\"blocks-gallery-item\"><figure><img loading=\"lazy\" width=\"800\" height=\"800\" src=\"http:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/Anatase_Reciprocal_wrongBand.png\" alt=\"\" data-id=\"965\" data-full-url=\"http:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/Anatase_Reciprocal_wrongBand.png\" data-link=\"http:\/\/www.calm-ebsd.com\/index.php\/news\/how-to-start\/manual-definition-of-bandwidths\/anatase_reciprocal_wrongband\/\" class=\"wp-image-965\" srcset=\"https:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/Anatase_Reciprocal_wrongBand.png 800w, https:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/Anatase_Reciprocal_wrongBand-300x300.png 300w, https:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/Anatase_Reciprocal_wrongBand-150x150.png 150w, https:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/Anatase_Reciprocal_wrongBand-768x768.png 768w, https:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/Anatase_Reciprocal_wrongBand-270x270.png 270w\" sizes=\"(max-width: 800px) 100vw, 800px\" \/><\/figure><\/li><\/ul><\/figure>\n\n\n\n<p>Selecting the pole (Ctrl+LMB) the <strong>band profile<\/strong> will be displayed in CALM. It is <strong>shown<\/strong> in the centered diagram <strong>by the white curve<\/strong> and does not really look like a reliable band profile. However, its <strong>1<sup>st<\/sup> derivative looks promising<\/strong> <strong>since<\/strong> the asymmetry of the extrema positions (green vertical lines) is with <strong>\u03b8<sub>asym<\/sub> = \u20120.018\u00b0<\/strong> very low. <strong>However<\/strong>, the resulting <strong>indexing<\/strong> of the diffracting lattice plane is quite high: <strong>(0 -15 7)<\/strong>, which <strong>indicates<\/strong> <strong>a big Bragg angle<\/strong> and a large distance of the reciprocal lattice point from the origin. <br>This is shown in the right image where this distance is so big that it is no more visible in this reciprocal latticeplane (uvw)*. There are already a few reciprocal lattice points, but <strong>this plane<\/strong> very likel <strong>does not match to this zone<\/strong>.<\/p>\n\n\n\n<p style=\"font-size:22px\">Correct description<\/p>\n\n\n\n<p>We can try a slightly different direction [hkl]* using <strong>two alternative great circles<\/strong> (red colored in the left image below). Since the solution was already found before &#8211; see the green circles around each [hkl]* &#8211; the indexing of the red colored [hkl]* is given in the band profile diagram and <strong>deliver<\/strong>s the diffracting lattice plane <strong>(0 -2 1)<\/strong>. <br>Also for this band, the white colored <strong>band profile<\/strong> is not much different to the former one and <strong>looks again<\/strong> quite <strong>awful<\/strong>. Neither the <strong>bigger \u03b8<sub>asym<\/sub> = \u20120.047\u00b0<\/strong> and the <strong>slightly lower I<sub>ampl<\/sub><\/strong> (derived maximum intensity) explain the preference of this solution compared to the upper one. <strong>However<\/strong>, the right image showing the zone in reciprocal space proves that both the <strong>direction and the distance<\/strong> between the two opposite reciprocal lattice points (bandwidth) <strong>perfectly match the translation lattice<\/strong> already found for this (uvw)*.   <\/p>\n\n\n\n<figure class=\"wp-block-gallery columns-3\"><ul class=\"blocks-gallery-grid\"><li class=\"blocks-gallery-item\"><figure><img loading=\"lazy\" width=\"382\" height=\"391\" src=\"http:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/correctPole.png\" alt=\"\" data-id=\"975\" data-full-url=\"http:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/correctPole.png\" data-link=\"http:\/\/www.calm-ebsd.com\/index.php\/news\/how-to-start\/manual-definition-of-bandwidths\/correctpole\/\" class=\"wp-image-975\" srcset=\"https:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/correctPole.png 382w, https:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/correctPole-293x300.png 293w, https:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/correctPole-264x270.png 264w\" sizes=\"(max-width: 382px) 100vw, 382px\" \/><\/figure><\/li><li class=\"blocks-gallery-item\"><figure><img loading=\"lazy\" width=\"503\" height=\"187\" src=\"http:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/correctBand.png\" alt=\"\" data-id=\"974\" data-full-url=\"http:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/correctBand.png\" data-link=\"http:\/\/www.calm-ebsd.com\/index.php\/news\/how-to-start\/manual-definition-of-bandwidths\/correctband\/\" class=\"wp-image-974\" srcset=\"https:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/correctBand.png 503w, https:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/correctBand-300x112.png 300w, https:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/correctBand-360x134.png 360w\" sizes=\"(max-width: 503px) 100vw, 503px\" \/><\/figure><\/li><li class=\"blocks-gallery-item\"><figure><img loading=\"lazy\" width=\"800\" height=\"800\" src=\"http:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/Anatase_Reciprocal.png\" alt=\"\" data-id=\"980\" data-full-url=\"http:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/Anatase_Reciprocal.png\" data-link=\"http:\/\/www.calm-ebsd.com\/index.php\/news\/how-to-start\/manual-definition-of-bandwidths\/anatase_reciprocal\/\" class=\"wp-image-980\" srcset=\"https:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/Anatase_Reciprocal.png 800w, https:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/Anatase_Reciprocal-300x300.png 300w, https:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/Anatase_Reciprocal-150x150.png 150w, https:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/Anatase_Reciprocal-768x768.png 768w, https:\/\/www.calm-ebsd.com\/wp-content\/uploads\/2021\/11\/Anatase_Reciprocal-270x270.png 270w\" sizes=\"(max-width: 800px) 100vw, 800px\" \/><\/figure><\/li><\/ul><\/figure>\n\n\n\n<p><em>This again emphasizes that lower band edge asymmetry or apparently higher band intensity are not inevitable criteria for the detection of a band. The only criterion is that the derived reciprocal lattice point must match those already present, or it forms a matching high-order sublattice.<\/em><\/p>\n\n\n\n<p>So <strong>be careful if only one lattice point<\/strong> occurs which <strong>forces a redefinition of all other lattice points<\/strong>.<\/p>\n","protected":false},"excerpt":{"rendered":"<p>It can happen that, by chance, exactly where a band could be, an intensity accumulation occurs that actually looks like a band profile. To make matters worse, most band profiles do not look as ideal as is commonly thought, but <a href=\"https:\/\/www.calm-ebsd.com\/index.php\/how-to-start\/false-bands\/\" class=\"read-more\">Read More &#8230;<\/a><\/p>\n","protected":false},"author":3,"featured_media":0,"parent":168,"menu_order":5,"comment_status":"closed","ping_status":"closed","template":"","meta":[],"_links":{"self":[{"href":"https:\/\/www.calm-ebsd.com\/index.php\/wp-json\/wp\/v2\/pages\/1000"}],"collection":[{"href":"https:\/\/www.calm-ebsd.com\/index.php\/wp-json\/wp\/v2\/pages"}],"about":[{"href":"https:\/\/www.calm-ebsd.com\/index.php\/wp-json\/wp\/v2\/types\/page"}],"author":[{"embeddable":true,"href":"https:\/\/www.calm-ebsd.com\/index.php\/wp-json\/wp\/v2\/users\/3"}],"replies":[{"embeddable":true,"href":"https:\/\/www.calm-ebsd.com\/index.php\/wp-json\/wp\/v2\/comments?post=1000"}],"version-history":[{"count":17,"href":"https:\/\/www.calm-ebsd.com\/index.php\/wp-json\/wp\/v2\/pages\/1000\/revisions"}],"predecessor-version":[{"id":1726,"href":"https:\/\/www.calm-ebsd.com\/index.php\/wp-json\/wp\/v2\/pages\/1000\/revisions\/1726"}],"up":[{"embeddable":true,"href":"https:\/\/www.calm-ebsd.com\/index.php\/wp-json\/wp\/v2\/pages\/168"}],"wp:attachment":[{"href":"https:\/\/www.calm-ebsd.com\/index.php\/wp-json\/wp\/v2\/media?parent=1000"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}